Asbestos fibre Counting by
Phase Contrast Microscopy
Methodology for PCM Analysis: NIOSH 7400 & OSHA ID160
Phase contrast microscopy is the method that is primarily used for estimating
asbestos concentrations of airborne fibres. This method is quick and can be
performed on-site for a rapid determination of concentrations of asbestos fibres
in the air. Phase contrast microscopy does not positively differentiate between
asbestos and other fibres. Positive identification of asbestos fibre must be
performed using PLM (Polarized Light Microscopy) or Electron Microscopy (Method
7402)
Required Microscope Equipment
Positive phase contrast microscope with 10X Brightfield and 40X Phase
objectives, GIF (Green Interference Filter), Walton & Beckett reticle Type-22G
and a stage micrometer with 0.01mm divisions.
Required
Test Slide
The HSE/NPL Mark II Phase Shift Test Slide checks or standardizes the visual
detection limits of the phase contrast microscope. The HSE/NPL Test Slide
consists of a conventional glass microscope slide with seven sets of parallel
line pairs of decreasing widths. The microscope must clearly resolve line pairs
1 thru 3. Line pairs 4 and 5 must be at least partially visible. Line pairs 6
and 7 must be invisible. A microscope which fails to meet these requirements is
either too low or too high in resolution and cannot be used for asbestos
detection.